Table of Peaks No. (ppm) (Hz) Height 1 3.25 1623.6 0.5035 2 3.26 1631.8 0.6051 3 3.27 1633.1 0.6322 4 3.28 1641.2 0.5300 5 3.39 1696.4 0.4601 6 3.41 1706.2 0.9323 7 3.43 1715.5 0.5949 8 3.55 1773.4 0.2971 9 3.56 1777.1 0.3451 10 3.56 1780.0 0.5675 11 3.57 1783.6 0.8360 12 3.58 1787.1 0.4911 13 3.58 1789.9 0.8844 14 3.59 1793.8 1.0000 15 3.60 1797.6 0.3212 16 3.60 1799.5 0.2868 17 3.61 1806.4 0.7426 18 3.63 1815.0 0.9166 19 3.65 1825.0 0.5318 20 3.66 1827.8 0.5672 21 3.67 1835.3 0.4148 22 3.68 1837.0 0.6662 23 3.69 1844.4 0.5720 24 3.69 1846.8 0.5578 25 3.70 1849.2 0.3220 26 3.70 1851.7 0.2523 27 3.71 1854.1 0.4583 28 3.71 1856.8 0.3120 29 3.72 1859.2 0.2709 30 3.73 1864.4 0.1288 31 3.73 1866.3 0.1456 32 3.74 1871.3 0.8485 33 3.75 1875.6 0.3060 34 3.75 1876.6 0.2804 35 3.76 1879.9 0.5844 36 3.76 1880.7 0.6453 37 3.77 1882.7 0.5318 38 3.77 1883.8 0.5651 39 3.77 1885.3 0.4284 40 3.78 1889.2 0.7581 41 3.79 1896.0 0.0863 42 3.81 1903.6 0.2187 43 3.82 1908.2 0.2315 44 3.83 1915.0 0.2741 45 3.84 1917.5 0.6786 46 3.84 1919.7 0.5334 47 3.86 1927.1 0.1210 48 3.86 1929.8 0.3519 49 3.87 1932.1 0.2773 50 3.89 1944.7 0.3115 51 3.89 1946.6 0.3164 52 3.92 1956.9 0.3379 53 3.92 1958.9 0.2825 54 3.93 1965.1 0.1035 55 3.94 1967.5 0.1228 56 3.94 1970.8 0.2970 57 3.96 1980.1 0.3117 58 3.98 1989.6 0.1943 59 5.22 2609.3 0.1255 60 5.23 2613.1 0.1441 61 5.40 2696.8 0.5586 62 5.40 2700.7 0.5208 Table of Multiplets No. Shift1 (ppm) Hs Type J (Hz) Atom1 Multiplet1 (ppm) 1 3.27 1 dd 9.46 8.08 10 M13 3.23 .. 3.30 2 3.41 2 t 9.55 5 M12 3.38 .. 3.45 3 3.58 4 m - 3 13 M11 3.54 .. 3.60 4 3.62 2 m - 8 M10 3.61 .. 3.64 5 3.66 2 m - 4 M09 3.64 .. 3.68 6 3.70 2 m - 6 M08 3.68 .. 3.73 7 3.76 4 m - 22 9 M07 3.73 .. 3.80 8 3.84 2 m - 17 M06 3.80 .. 3.88 9 3.90 1 dd 12.27 1.92 22 13 M05 3.88 .. 3.92 10 3.93 1 d 2.38 M04 3.92 .. 3.94 11 3.96 1 m - 9 M03 3.94 .. 3.99 12 5.22 1 d 3.80 11 M02 5.21 .. 5.24 13 5.40 1 d 3.89 2 M01 5.38 .. 5.42 Table of Assignments No. Atom Exp. Shift (ppm) Multiplet 1 10 3.27 M13 2 5 3.41 M12 3 3 3.58 M11 4 13 3.58 M11 5 8 3.62 M10 6 4 3.66 M09 7 6 3.70 M08 8 22 3.76 M07 9 9 3.76 M07 10 17 3.84 M06 11 22 3.90 M05 12 13 3.90 M05 13 9 3.96 M03 14 11 5.22 M02 15 2 5.40 M01